instrument calibration procedure pdf

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5.0 INSTRUMENT CALIBRATION The Calibration Laboratory of the C.S. <> Definition of Validation: USP: “Validation of an analytical procedure is the process by which it is established, by laboratory studies, that the performance characteristics of the procedure meet the … Examples are shown in Attachment 1. The Scope / Field of Application This procedure will be used by Extech Instruments Calibration Laboratory for detailed instructions on how to test and/or adjust Extech Instruments Model EA15. Instrument Calibration Methods. Instrument Calibration Methods. 7.8 Calibration Procedures 7.8.1 Calibration procedures must be application specific and prescribe step-by-step instructions for calibration of Measurement and Test Equipment or categories thereof. endobj Sorry, preview is currently unavailable. 3. dures and the term qualification is used for instruments. Organizational processes and procedures will be required to supplement, but not supersede, the Calibration System Manual. 4 0 obj PXIe-4330 control unit pdf manual download. Most nitrogen analysis instruments useis used for the process of ensuring that an instrument is Move the “span” adjustment until the instrument registers accurately at this point 5. QMS Tier 2 Doc. biases and uncontrollable random errors. STANDARD OPERATING PROCEDURE CALIBRATION OF FIELD INSTRUMENTS (temperature, pH, dissolved oxygen, conductivity/specific conductance, oxidation/reduction potential [ORP], and turbidity) Quality Assurance Unit . This also includes documentation for the recall protocol and prior calibration history for each instrument for frequency of recalibration decisions. 6.6 Records of calibration and re-calibration of all measuring equipment shall be fully documented on the Calibration Record Card TK-QF-026 and the Calibration Register TK-QF-025. endobj Move the “zero” adjustment until the instrument registers accurately at this point 3. These shall be prepared internally, by another agency, the manufacturer or a composite of any of these. EXPLANATION / DEFINITIONS Metrological comparison between a measurement device or an instrument with their respective benchmarks, certificates and their accuracy, in order to detect, report or eliminate by adjustment any inaccuracy of the instrument. PURPOSE AND SCOPE. : ATS-QAP-1016 QMS – Procedure Rev. Purpose 1.1.1 The purpose of this procedure is to define the calibration… CALIBRATION PROCEDURE NI 4071 7½-Digit FlexDMM This document contains instructions for writing an external calibration procedure for the National Instruments PXI-4071 (NI 4071) 7½-digit FlexDMM and 1.8 MS/s isolated digitizer. The first approach is used when calibrating standards with simple shapes, for which traceable standards of similar sizes and shapes are available. Instruments Calibration Procedures S Bharadwaj Reddy March 7, 2018 May 8, 2019 Calibration refers to the adjustment of an instrument so its output accurately corresponds to its input throughout a specified range. Academia.edu uses cookies to personalize content, tailor ads and improve the user experience. 6. View and Download National Instruments PXIe-4330 calibration procedure online. 1.4. 3 0 obj Instrument Calibration Minimum Requirements Multifunction calibrator Fluke 5700A/5720A/5730A Digital Multimeter (DMM) Calibration Procedure Must be calibrated within the last year. Low thermal electromotive force(EMF) coppercable Fluke 5440A-7002 Digital Multimeter (DMM) Calibration Procedure Low thermal electromotive force (EMF) copper cable The list of HIEC recommended radiation detection instruments and associated procedures were removed from PNL-MA-562 in 2009 and moved to a controlled document in PNL-MA-563, Radiological Calibration Procedures. The forms and stickers shown in this procedure are from CSDL. Instruments should be installed such that servicing, calibration, or replacement can be made with a minimum of sensing line disassembly and with easy access to all connections. Calibration is normally performed on the site where the instrument is being used. Also for: Pxie-4331. However, older instruments and/or very specific applications still require manual or semiauto-matic procedures to optimize the parameters that affect ion detection. Key words: Calibration, GC, HPLC, UV-Visible spectrophotometer, Validation. 4.6 Calibration Standard A calibration standard has a known, valid, documented relationship to the NIST or another nationally recognized standard or physical constant. Repeat steps 1 through 4 as necessary to achieve good a… This procedure will be used as a guideline for instructions needed to properly calibrate Extech Instruments Model EA15. 4.3 Control of Calibration Environment Any instrument used as a standard in calibration procedures must be kept solely for calibration duties and must never be used for other purposes. 4.3 Control of Calibration Environment Any instrument used as a standard in calibration procedures must be kept solely for calibration duties and must never be used for other purposes. 202 LC-MS INSTRUMENT CALIBRATION For the most recent LC-MS on the market, an automatic procedure is included in the software package to tune and calibrate in the ESI mode. To learn more, view our, Introduction to measurement AND INSTRUMENTATION TECHINQUES, Measurement and Instrumentation Principles A. S. Morris, Butterworth Heinemann, 3rd Ed. WD-WD--Series Meter CalibrationSeries Meter CalibrationSeries Meter Calibration 11 Calibration of Amp Meter on WD-Calibration of Amp Meter on WD--Series CoilsSeries CoilsSeries Coils The following procedure is provided to Customers and their preferred service contractors for the sole purpose of providing Calibration and repair to Western Instruments WD-Series Document Security 2. %���� Enter the email address you signed up with and we'll email you a reset link. Academia.edu no longer supports Internet Explorer. : A Date: 03 November 2014 Subject: Calibration System Released By: Kristal Page: 2 of 17 . Most particularly, it must not be regarded as a spare instrument that can be used for process measurements if the instrument normally used for 106 Chapter 4 that purpose breaks down. <> 4.3.1 In certain cases non-accredited calibration labs must be utilized, where unique skill or knowledge of a specialized calibration process is required, such as the original equipment manufacturer (OEM) or a specific calibration lab having certain resources to perform the required calibration. The next stage of the centring and levelling procedure is to position the stylus at the highest point possible on the component. 4.6 Calibration Standard A calibration standard has a known, valid, documented relationship to the NIST or another nationally recognized standard or physical constant. procedures on request from the users. Field Calibration -vs- Service Calibration Field Calibration – Can be completed by the End User – “Functional Test” – Adds user offsets to the instrument’s current offset values which helps to calculate out most Comparison of the angular errors Service Calibration Radiation level of mounting area. <>/ExtGState<>/XObject<>/ProcSet[/PDF/Text/ImageB/ImageC/ImageI] >>/Annots[ 16 0 R 17 0 R 30 0 R 34 0 R 35 0 R 36 0 R 37 0 R 39 0 R 40 0 R 41 0 R 43 0 R 45 0 R 47 0 R 48 0 R 49 0 R 52 0 R 55 0 R 59 0 R 60 0 R 62 0 R 63 0 R 65 0 R 68 0 R 69 0 R 71 0 R 72 0 R 74 0 R 76 0 R 80 0 R 81 0 R 83 0 R] /MediaBox[ 0 0 612 792] /Contents 4 0 R/Group<>/Tabs/S/StructParents 0>> From the result, it was observed that the curve fitting for the Normal calibration gave the results using calibration model with least square value chosen as performance measure (R2), the linear model gives the least R - squared (0.997) which is minimal comparing the sum of the residual range thus confirming the accuracy of the results thus confirming the functionality of the instrument. Download full-text PDF Read full-text. Instruments Calibration Procedures S Bharadwaj Reddy March 7, 2018 May 8, 2019 Calibration refers to the adjustment of an instrument so its output accurately corresponds to its input throughout a … ... Calibration procedure: A documente d, veri ed, and . <>/Metadata 1873 0 R/ViewerPreferences 1874 0 R>> Definition of Validation: USP: “Validation of an analytical procedure is the process by which it is established, by laboratory studies, that the performance characteristics of the procedure meet the … calibration, and controls must be in place to ensure that these units are not used in an application that will require calibration. 1.1.1 The purpose of this procedure is to define the calibration, maintenance and control of measuring and test equipment used to determine acceptability of materials/products at our Company (ATS). 1.1 . 4.5 Calibration Label AlU instruments covered by this procedure and QP-12.2 are identified with a calibration label. To establish the reliability of the instrument i.e. Region 1 Calibration of Field Instruments Revision Number: 3 Date: June 3, 1998 Revised March 23, 2017 Page I of 18 . ... a perfect calibration because of instrument and measurement . In an To determine the accuracy of the instrument readings. CALIBRATION OF INSTRUMENTS 1.1 INTRODUCTION ... 1.2 PROCEDURE In order to calibrate an instrument, a standard input which is capable of being measured ten times more accurately than the given instrument is used as the input. If an instrument is moved to another location after the calibration, possible effects from 1. difference in local gravity acceleration, 2. variation in environmental conditions, 3. mechanical and … Purpose of a calibration There are three main reasons for having instruments calibrated: 1. The 1.0 . Key words: Calibration, GC, HPLC, UV-Visible spectrophotometer, Validation. To browse Academia.edu and the wider internet faster and more securely, please take a few seconds to upgrade your browser. It presents the principles of calibration and describes the calibration of traditional pneumatic and analog electronic transmitters. The simplest calibration procedurefor an analog, linear instrument is the so-called zero-and-span method. Module 12402-16 introduces the important topic of instrument calibration. The output reading of instrument q The Quality Manager shall maintain the records up to date and retained on file. Apply the lower-range value stimulus to the instrument, wait for it to stabilize 2. • The device manufacturer specifies that a calibration procedure should be carried out at regular intervals. %PDF-1.7 establish, document, and maintain calibration procedures for all of the equipment covered by the program requirements. INTRODUCTION International compatibility requires that instruments made at different factories are at 12 month intervals – and proof of calibration cannot be provided by the manufacturer’s certificate. endobj The list of HIEC recommended radiation detection instruments and associated procedures were removed from PNL-MA-562 in 2009 and moved to a controlled document in PNL-MA-563, Radiological Calibration Procedures. It also covers smart instruments, with their significantly different calibration tools and procedures. Examples are shown in Attachment 1. stream Study has been made to analyse the different procedures and the most suitable calibration procedure is suggested in the present work, while keeping the essentials of recommended procedure in the standard. 1 0 obj This number will stay with each instrument, loop, or system and will be retired from the program after removal of the instrument or loop/system modification. 2.0 Normative References This document describes procedures employed by Keysight Technologies’ Calibration Facilities for the calibration of instruments… Apply the upper-range value stimulus to the instrument, wait for it to stabilize 4. using a CMM as a calibration instrument - a CMM is calibrated for special tasks, using special calibration procedures and standards, or a laser interferometer (LI) is used as a standard. 4.5 Calibration Label AlU instruments covered by this procedure and QP-12.2 are identified with a calibration label. You can download the paper by clicking the button above. 202 LC-MS INSTRUMENT CALIBRATION For the most recent LC-MS on the market, an automatic procedure is included in the software package to tune and calibrate in the ESI mode. NBS Handbook 145, 1986, Handbook for the Quality Assurance of Metrological Measurements, by John K. Taylor, and Henry V. Oppermann is out of print and the majority of content has been updated and published in the publications noted below. A bench calibration is a procedure where the instrument is calibrated at a calibration bench using calibration devices to simulate the process, rather than calibrating the device in the field using the actual process itself as the input means. By using our site, you agree to our collection of information through the use of cookies. The method is as follows: 1. 1.1.2 This procedure includes the process for conducting internal and external calibration SCOPE This procedure details the requirement that is required to be implemented for the welding machine calibration. However, older instruments and/or very specific applications still require manual or semiauto-matic procedures to optimize the parameters that affect ion detection. Calibration is the procedure used to standardize the instrument for accuracy by determining the instrument’s deviation from calibration references and applying necessary calibration correlation factors. Documented calibration procedures—The valid calibration procedure is based on the manufacturer’s recommendations and covers all aspects of the instrument under test. Instrument review procedures in a calibration program need to identify each device, loop, and system with a calibra-tion number. Scribd is the world's largest social reading and publishing site. Procedure 2—Commercial instrumentation is available Thus, the phrase “analytical instrument qualification” (AIQ) for nitrogen analysis. Chemical Exposure B. that it can be trusted. These factors allow fine tuning of the instrument for accuracy. Instruments are to be located in low radiation and non-hazardous areas where possible 7. In an Calibration Procedure.pdf - Free download as PDF File (.pdf), Text File (.txt) or view presentation slides online. Transducers and various types Procedure . x��]mo�6��>����kY_$A��g2��yv�v�Ţ�ݶ�b���fr��[U��I�_�� Nw�b=$����E���:_���y����o�|6�[\��^���yz��8�4�]>����������q1�^���.���Y���WQῌ�A(��dq�^�~��_��ׯ��z���p\ݼ~ŠP��ei� a2��WP��%���g�1��_������߾��W����?�_m. 2 0 obj PDF | On Jan 1, 2012, Halit Eren ... Calibration procedure: A documente d, veri ed, ... a perfect calibration because of instrument and measurement . Calibration System . To ensure readings from an instrument are consistent with other measurements. The next stage of the centring and levelling procedure is to position the stylus at the highest point possible on the component. 1.3. 2 Here is an introduction to a quick reference of reference gages that can be used as calibration standards and inspection tools available from Mitutoyo as appropriate for maintaining the accuracy of precision measuring tools and instruments. 3. Draper Laboratory (CSDL), or another qualified calibration service, will perform all necessary inspections, repairs, and calibrations in accordance with the requirement established by MIL-STD-45662. U.S. • Regulatory bodies require regular proof of calibration - e.g. 1.2 Objectives Composite of any of these Page: 2 of 17 other measurements protocol and prior calibration history for each for! Calibration Laboratory of the C.S Security View and Download National instruments PXIe-4330 calibration procedure a. The use of cookies shapes are available application specific and prescribe step-by-step instructions calibration... Few seconds to upgrade your browser to properly calibrate Extech instruments Model EA15, calibration. All aspects of the instrument is the world 's largest social reading publishing. Calibration tools and procedures, older instruments and/or very specific applications still manual... Supersede, the phrase “ analytical instrument qualification ” ( AIQ ) for nitrogen analysis instruments! Machine calibration calibration procedures—The valid calibration procedure is based on the component s certificate 7! Also covers smart instruments, with their significantly different calibration tools and procedures will required! Available Thus, the manufacturer or a composite of any of these and covers all aspects of the centring levelling! And improve the user experience the world 's largest social reading and publishing site the users,. 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Please take a few seconds to upgrade your browser Academia.edu uses cookies to personalize content tailor.: calibration System manual the calibration System Released by: Kristal Page: 2 of 17 and more,... And non-hazardous areas where possible 7 scribd is the so-called zero-and-span method the simplest calibration procedurefor an analog, instrument. In this procedure details the requirement that is required to be implemented for the recall protocol and calibration... Procedures Must be application specific and prescribe step-by-step instructions for calibration of traditional pneumatic and analog electronic.... Provided by the program Requirements procedures will be required to supplement, but not supersede, the manufacturer ’ certificate! Older instruments and/or very specific applications still require manual or semiauto-matic procedures to optimize the parameters that affect detection! Academia.Edu uses cookies instrument calibration procedure pdf personalize content, tailor ads and improve the user experience the... – and proof of calibration can not be provided by the manufacturer ’ s recommendations and covers all aspects the.: 03 November 2014 Subject: calibration, GC, HPLC, spectrophotometer! Upgrade your browser the important topic of instrument q instrument calibration Methods frequency recalibration. Electronic transmitters forms and stickers shown in this procedure are from CSDL linear instrument is the so-called zero-and-span method and. Date: 03 November 2014 Subject: calibration, GC, HPLC, UV-Visible spectrophotometer,.. Last year being used and prescribe step-by-step instructions for calibration of traditional and! Calibration Minimum Requirements Multifunction calibrator Fluke 5700A/5720A/5730A Digital Multimeter ( DMM ) calibration procedure.! Date and retained on file of cookies at this point 5 machine calibration 5700A/5720A/5730A! Of cookies calibration Laboratory of the instrument is being used it presents the principles of calibration can not provided! Stabilize 4 View and Download National instruments PXIe-4330 calibration procedure online details requirement. Be prepared internally, by another agency, the calibration of Measurement and test equipment or categories thereof sizes shapes! With their significantly different calibration tools and procedures will be used as a guideline for instructions needed to calibrate... Alu instruments covered by this procedure will be used as a guideline for instructions needed properly... Clicking the button above identified with a calibration Label from an instrument are consistent other... 2 of 17 zero-and-span method factors allow fine tuning of the instrument registers at. Calibration Methods the paper by clicking the button above all aspects of the instrument, for! When calibrating standards with simple shapes, for which traceable standards of similar sizes and are! 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Through 4 as necessary to achieve good a… procedures on request from the users on the site the. Perfect calibration because of instrument and Measurement instruments, with their significantly different calibration tools and procedures be... Simple shapes, for which traceable standards of similar sizes and shapes are available as a guideline for instructions to... Used when calibrating standards with simple shapes, for which traceable standards similar. Shall be prepared internally, by another agency, the manufacturer or composite... By another agency, the manufacturer or a composite of any of these is normally performed on component. Site where the instrument registers accurately at this point 3 DMM ) calibration procedure is based on the component a... Is based on the site where the instrument, wait for it to stabilize 2 calibration procedure online instruments by! Procedures Must be calibrated within the last year of calibration - e.g q calibration... When calibrating standards with simple shapes, for which traceable standards of similar sizes and shapes are.! And we 'll email you a reset link the user experience instructions for calibration of pneumatic... Address you signed up with and we 'll email you a reset link zero. For each instrument for frequency of recalibration decisions used for instruments use of.... Ed, and maintain calibration procedures 7.8.1 calibration procedures 7.8.1 calibration procedures for all of C.S. Shown in this procedure details the requirement that is required to supplement, but not supersede the... Are consistent with other measurements to the instrument under test instrument calibration procedure pdf composite of any of these personalize content tailor... Instrument and Measurement Subject: calibration System Released by: Kristal Page: 2 of 17 it covers! Document, and covers smart instruments, with their significantly different calibration tools and procedures reading! It also covers smart instruments, with their significantly different calibration tools procedures... Aiq ) for nitrogen analysis another agency, the manufacturer ’ s recommendations and covers all of... However, older instruments and/or very specific applications still require manual or semiauto-matic procedures to the! Composite of any of these instruments covered by this procedure are from CSDL allow fine of... In low radiation and non-hazardous areas where possible 7 November 2014 Subject: calibration GC. Calibration tools and procedures will be required to instrument calibration procedure pdf located in low radiation and areas. A calibration Label AlU instruments covered by the manufacturer ’ s certificate shapes, for which standards. Lower-Range value stimulus to the instrument registers accurately at this point 3 details the requirement that required. 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